Contents
1.0 Introduction
2.0 Process Characteristics
2.1 Reaction Chemistry
2.2 Process Engineering Constraints
3.0 Control Configurations
3.1 Direct Jacket Heat/Cool
3.2 Direct Jacket Cool/Indirect Heat
3.3 Indirect Jacket Heat/Cool
3.4 Instrumentation and Control
4.0 Performance Predictions
Appendices
I Summary of Heat Transfer in Glass Lined Reactors
(Acknowledgements to Pfaudler Reactor Systems)
II Control Valve Characteristic Selection
III Control Loop Tuning
IV ChemCAD User Guidance Notes
Figures
1. Reactor Control Systems
2. Indirect Jacket Heating Model
3. Indirect Jacket Cooling Model
4. Condenser Control System
5. Condenser Control System Model
6. Control Valve Characteristics
7. Controller & Control Valve Action (ChemCAD)
8. Reactor Thermal Rating Spreadsheet
9. Batch Reactor Plot Options
Graphs
1. 1600L Hastelloy Reactor Heat Up
2. 1600L Reactor Boil Up/Emissions
3. 1600L Hastelloy Reactor Cool Down
4. Condenser Model Controller Tuning Tu
5. Condenser Model Controller Tuning
Process Modelling and Control of
Batch Reactors in the Fine Chemicals Industry

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